﻿<?xml version="1.0"?>
<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/2.2" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/2.2 http://www.xrdml.com/XRDMeasurement/2.2/XRDMeasurement.xsd" status="Completed" recordIdentifier="{3ECC8CC9-E033-4470-83C8-302DC0184543}">
	<comment>
		<entry>Configuration=Conf. Chi-Phi-z stage + motorized Double Tilt, Owner=schlomgroup, Creation date=5/2/2023 6:11:30 AM</entry>
		<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
		<entry>Sample stage=Chi-Phi-z stage 240 mm (reflection); Minimum step size Phi:0.01; Minimum step size Chi:0.01; Minimum step size Z:0.001</entry>
		<entry>Diffractometer system=EMPYREAN</entry>
		<entry>Measurement program=Manual, Created by=schlomgroup, Id=WL:DESKTOP-CG4UMQ1:schlomgroup, Creation date=1/16/2024 3:13:55 PM</entry>
	</comment>
	<sample type="To be analyzed">
		<id></id>
		<name></name>
		<preparedBy></preparedBy>
	</sample>
	<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
		<comment>
			<entry>PHD Lower Level = 5.63 (keV), PHD Upper Level = 12.88 (keV)</entry>
		</comment>
		<usedWavelength intended="K-Alpha 1">
			<kAlpha1 unit="Angstrom">1.5405980</kAlpha1>
			<kAlpha2 unit="Angstrom">1.5444260</kAlpha2>
			<kBeta unit="Angstrom">1.3922500</kBeta>
			<ratioKAlpha2KAlpha1>0.0000</ratioKAlpha2KAlpha1>
		</usedWavelength>
		<incidentBeamPath>
			<radius unit="mm">240.00</radius>
			<xRayTube id="1010048" name="Empyrean Cu LFF HR (9430 033 7310x) DK433060">
				<tension unit="kV">45.0</tension>
				<current unit="mA">40.0</current>
				<anodeMaterial>Cu</anodeMaterial>
				<focus type="Line">
					<length unit="mm">12.0</length>
					<width unit="mm">0.4</width>
					<takeOffAngle unit="deg">4.4</takeOffAngle>
				</focus>
			</xRayTube>
			<xRayMirror id="27080001" name="Inc. Beam Cu W/Si (hybrid MPD)" hybrid="true">
				<crystal type="Graded" shape="Parabolic">W/Si</crystal>
				<acceptanceAngle unit="deg">0.800</acceptanceAngle>
				<length unit="mm">55.3</length>
			</xRayMirror>
			<monochromator id="23090002" name="Hybrid monochr. 2xGe220 Cu asym." hybrid="true">
				<crystal type="Asymmetric" shape="Flat">Ge</crystal>
				<numberOfReflections>2</numberOfReflections>
				<hkl>
					<h>2</h>
					<k>2</k>
					<l>0</l>
				</hkl>
			</monochromator>
			<divergenceSlit id="22010011" name="Fixed slit 1/32°" xsi:type="fixedDivergenceSlitType">
				<distanceToSample unit="mm">179.30</distanceToSample>
				<height unit="mm">0.05</height>
			</divergenceSlit>
		</incidentBeamPath>
		<diffractedBeamPath>
			<radius unit="mm">240.00</radius>
			<detector id="7010020" name="PIXcel3D-Medipix3 1x1 detector" xsi:type="areaDetectorType">
				<phd unit="%">
					<lowerLevel>35.0</lowerLevel>
					<upperLevel>80.0</upperLevel>
				</phd>
				<mode>Receiving slit</mode>
				<activeChannelsEquatorial>3</activeChannelsEquatorial>
				<activeChannelsAxial>255</activeChannelsAxial>
				<pitchEquatorial unit="mm">0.05500</pitchEquatorial>
				<pitchAxial unit="mm">0.05500</pitchAxial>
				<readOutPeriod unit="seconds">0.050</readOutPeriod>
			</detector>
		</diffractedBeamPath>
		<scan appendNumber="0" mode="Continuous" scanAxis="2Theta-Omega" status="Completed">
			<header>
				<startTimeStamp>2024-01-16T15:15:35-05:00</startTimeStamp>
				<endTimeStamp>2024-01-16T15:16:39-05:00</endTimeStamp>
				<author>
					<name>schlomgroup</name>
				</author>
				<source>
					<applicationSoftware version="7.2a">Data Collector</applicationSoftware>
					<instrumentControlSoftware version="8.2  20201204">EMPYREAN</instrumentControlSoftware>
					<instrumentID>0000000011261638</instrumentID>
				</source>
			</header>
			<scanAxisCenter>
				<position axis="2Theta" unit="deg">3.0000</position>
				<position axis="Omega" unit="deg">1.5000</position>
			</scanAxisCenter>
			<reflection>
				<hkl>
					<h>0</h>
					<k>0</k>
					<l>0</l>
				</hkl>
			</reflection>
			<dataPoints>
				<positions axis="2Theta" unit="deg">
					<startPosition>0.0100</startPosition>
					<endPosition>5.9900</endPosition>
				</positions>
				<positions axis="Omega" unit="deg">
					<startPosition>0.0050</startPosition>
					<endPosition>2.9950</endPosition>
				</positions>
				<positions axis="Phi" unit="deg">
					<commonPosition>0.00</commonPosition>
				</positions>
				<positions axis="Chi" unit="deg">
					<commonPosition>0.00</commonPosition>
				</positions>
				<positions axis="Z" unit="mm">
					<commonPosition>6.604</commonPosition>
				</positions>
				<commonCountingTime unit="seconds">0.088</commonCountingTime>
				<counts unit="counts">617416 640173 433099 227423 94792 45098 36118 38154 42082 46092 49422 53871 57892 61115 64738 68715 71845 75128 79662 83650 86544 90840 94062 97455 101182 103932 108337 111051 114131 118631 121038 124521 127306 128590 132771 134367 136693 141835 143337 146631 149424 152534 155937 155570 159364 161172 163122 167218 167870 170603 172999 172743 174283 174369 175247 177178 177952 179207 179708 179147 181870 181793 179201 177703 175182 175260 170332 166450 162430 157135 152693 144758 136521 129006 120643 114048 106183 95789 88931 78590 72642 63433 54757 48344 41437 36079 30923 26346 22979 19497 17249 15208 13514 12555 11607 11402 11047 10891 10845 10837 10883 10933 10754 10926 11178 11030 11000 10557 10360 9959 9720 9321 8890 8399 8045 7501 7318 6679 6293 5935 5196 4854 4631 3966 3728 3307 3142 2715 2376 2333 2100 1824 1785 1649 1525 1471 1455 1505 1482 1397 1512 1490 1571 1569 1612 1669 1674 1751 1694 1739 1740 1763 1743 1761 1749 1732 1664 1658 1632 1538 1476 1404 1401 1275 1219 1207 1133 1011 937 867 823 714 703 596 543 506 450 416 402 344 340 297 270 249 264 254 262 257 292 263 264 301 299 285 349 323 327 361 362 406 370 360 354 403 391 392 380 356 364 376 366 343 348 314 289 264 252 256 236 228 201 174 174 175 136 134 115 91 87 73 62 68 73 48 55 50 47 47 49 41 46 55 72 65 61 62 74 64 74 77 77 105 88 100 100 100 93 94 106 101 94 100 93 97 88 85 82 86 72 74 64 57 42 50 49 44 42 36 29 26 33 23 17 19 19 19 20 8 11 15 9 13 11 9 11 15 14 16 12 24 17 21 26 23 20 19 35 26 20 30 36 32 44 29 37 31 23 38 21 24 35 26 24 21 33 13 14 16 21 11 11 7 12 15 5 7 5 5 8 3 3 5 5 3 3 2 1 1 1 3 5 4 6 8 9 11 8 5 10 11 8 7 1 6 10 11 18 10 5 13 14 6 11 9 11 5 9 9 4 7 8 5 3 2 4 4 3 3 2 4 4 3 3 4 4 2 2 2 0 1 2 3 3 7 1 2 3 5 4 7 4 1 8 3 4 7 4 2 4 1 1 5 2 5 3 6 2 2 7 3 2 2 3 7 2 2 3 3 4 2 3 2 3 0 2 1 0 1 2 2 1 3 2 2 1 3 3 2 1 2 1 1 1 4 1 3 3 0 4 3 0 0 3 3 1 0 3 2 1 3 0 3 3 2 1 0 1 4 4 1 0 1 1 2 1 1 1 0 0 0 2 1 0 1 0 1 1 1 0 0 0 0 1 1 0 1 2 0 1 1 1 1 1 2 3 1 0 1 3 1 5 0 4 1 0 0 1 0 1 0 0 0 0 1 2 1 3 0 1 1 0 2 0 1 0 1 0 0 1 1 1 1 0 1 0 0 0 1 2 1 1 0 1 1 2 0 0 1 2 1 2 1 1 1 2 0 0 2 1 2 1 0 1 2 1 3 0 0 0</counts>
			</dataPoints>
		</scan>
	</xrdMeasurement>
</xrdMeasurements>
